With a range of characteristics such as fluid, sheet and powder, their complex balance needs to be assessed, controlled and observed before, during and after assembly.

Lithium-ion battery materials are highly sensitive to air exposure. It’s not feasible to establish an assembly line where the product is isolated from the atmosphere, therefore a glovebox is used that ensures the material is not fragilized during the analysis process.

Several factors are significant in this complex process and we can provide the solution you need.

  • Fine Raw material structure (down to the atomic level)
  • Power coating thickness
  • Internal structure and elemental distribution mappings
  • Homogeneity of solid state electrodes
  • 3D volume analysis
  • Chemical analysis if SEM is not enough

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Find more in-depth information and advice in our brochure on scanning electron microscopy and surface analysis for batteries.
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Sample preparation equipment for clear structural analysis

Active material particules

  • Sizing & Shapes
  • Outer grain structrure
  • Surface coating

Electrodes 

  • Topography
  • Foreign matter

Separator 

  • Fibril & pore structure
  • Foreign matter
  • Ceramics coating damage
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Cathode observed on FE-SEM SU5000

Low-kV study of coating homogenity
on cathode particle.

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Anode Inspection observed on W-SEM FlexSEM 1000 II

Foreign particle inclusions

Critical, as they might punch separators and
cause failure.

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Separator observed on FE-SEM

Separators exhibit very beam-sensitive ultra-fine fibril structures, which are easily altered or damaged during SEM inspection, Serial Frame Capture allows proper image.

Product spotlight IM5000

The most advanced broad ion beam system for producing exceptionally high-quality cross-section or flat-milling samples for electron microscopy. Widths up to 8 mm with milling rate: 1 mm/hour.

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High performance ion milling systems for incredible results with cross section analysis

Active material particle
Inner structure

  • Grainpores, cracks, core-shell structure (anti-corrosion)

Separator

  • Inner structure, layer thickness

Electrodes

  • Geometrical structure (filling, porosity, cracks, binder distribution, rolling damage) aging analysis
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Cross Section of Cathode

Prepared with IM5000 in less than one hour. Observed with FE-SEM SU7000.

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Cross Section of Separator

Using Cryo Temperature Control of IM5000, layer thicknesses and fibril structures are maintained.
Observed with Cold FE-SEM.

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Cross Section of Anode

Prepared with IM5000.
Observed with FE-SEM SU7000.

CS-Seperator-2.jpg

Product spotlight IM4000 II

IM4000II supports both cross section milling and/or flat-milling to prepare specimens depending on the purpose. Cooling Temperature Control, Air Protection Holder Unit, and Various options enable preparation of various cross section specimens.

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How can we help you?

Get great, friendly, free advice from our expert team of technologists and engineers.

Discover Air Protection Solution

For specimen exchange, discover the advantages of air protected transfer for processing & observation workflow

MET 200kV

HF5000

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Ion Milling System

ArBlade 5000

 

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FE-SEM

SU7000

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SEM

SU3900

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FIB

ETHOS NX5000

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Technical Support

When you need technical support, we’ll give it to you – the best there is. Fast, reliable, skilled and experienced, you can trust us to provide the right answers and the best solutions.

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